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Three-dimensional in situ observations of short fatigue crack growth in magnesium

机译:镁短疲劳裂纹扩展的三维原位观察

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摘要

Three-dimensional (3D) short fatigue crack growth behaviour in a cast magnesium alloy, Elektron 21, was studied using a combination of X-ray diffraction contrast tomography (DCT) and microtomography at the European Synchrotron Radiation Facility. A 3D map of grain shapes and crystallographic orientations was produced in a miniature fatigue specimen using DCT. A focused ion beam instrument was used to introduce small notches in selected grains. Synchrotron microtomography was used to study the evolution of fatigue cracks from these notches during interrupted in situ fatigue cycling. Stage I crack growth occurred preferentially on the basal plane of the magnesium hexagonal close packed crystal, with local crack growth rates between 4 and 40 nm cycle. Retardations in the local crack growth rate were observed in certain grains and at certain grain boundaries. The observed interactions between the crack and the polycrystalline microstructure can be explained using Schmid factors and a development of the tilt-twist model of Zhai and Wilkinson (Zhai T, Wilkinson AJ, Martin JW. Acta Mater 2000;48;4917). Copyright 2011 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
机译:在欧洲同步辐射装置上,结合使用X射线衍射对比断层扫描(DCT)和显微断层摄影技术,研究了铸造镁合金Elektron 21中的三维(3D)短疲劳裂纹扩展行为。使用DCT在微型疲劳样品中生成了晶粒形状和晶体取向的3D图。使用聚焦离子束仪器在选定的晶粒中引入小缺口。同步辐射显微断层照相术用于研究在原位疲劳循环中断期间这些缺口产生的疲劳裂纹。第一阶段的裂纹扩展优先发生在镁六方密堆积晶体的基面上,局部裂纹扩展速率在4至40 nm周期之间。在某些晶粒和某些晶界观察到局部裂纹扩展速率的降低。可以使用Schmid因子和Zhai和Wilkinson的倾斜扭曲模型的发展来解释观察到的裂纹与多晶微结构之间的相互作用(Zhai T,Wilkinson AJ,Martin JW。Acta Mater 2000; 48; 4917)。版权所有2011 Acta Materialia Inc.,由Elsevier Ltd.发行。保留所有权利。

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